# The Effects of Anisotropic Insulations with Different Spatial Distributions on Material Properties of Mortar Specimens

- Sang-Yeop Chung
^{1}, - Mohamed Abd Elrahman
^{1, 2}Email author and - Dietmar Stephan
^{1}

**11**:218

https://doi.org/10.1007/s40069-017-0218-3

© The Author(s) 2017

**Received: **25 August 2016

**Accepted: **23 October 2017

**Published: **7 December 2017

## Abstract

Insulating concrete is a material designed to reduce heat conduction with pores/insulations, and these pores strongly affect the material characteristics. In general, the insulation effect is directly proportion to the pore volume, while the material strength decreases as the porosity increases. To overcome this contrary, anisotropic insulations with different spatial distributions are proposed and investigated in this study. A set of mortar specimens with different arrangements of coin-shaped insulations are produced to examine the anisotropic insulation effect on the material characteristics. In addition, different types of insulation materials and their effect on the materials are also investigated here. X-ray computed tomography images and probabilistic description methods are used to confirm the arrangement of the insulations. The thermal and mechanical responses for different directions are investigated using both experimental and numerical methods. From the results, it is demonstrated that the use of anisotropic insulations for a specific direction can enhance the insulation efficiently as well as minimizing the loss of compressive strength.

## Keywords

## 1 Introduction

In recent years, energy consumption is considered as a serious problem in many engineering fields, and many efforts have been conducted to improve energy efficiency. Many new buildings and construction materials have been suggested and used over the last decades (Roma-Jr and Martello 2008; Sales et al. 2010; Benmansour et al. 2014). In particular, insulating concrete has been widely used to reduce energy consumption. Insulating concrete is a material designed to enhance insulation effect by using insulating components, such as lightweight aggregates, and entrained pores. The type of insulation contained in the specimen and its characteristics play a significant role in reducing heat transfer and material properties of insulating concrete (Narayanan and Ramamurthy 2000; Baetens et al. 2011; Chabannes et al. 2014; Binici et al. 2016).

Insulating concrete contains numerous pores inside the material, and the volume ratio and the spatial distribution of these insulations strongly affect the characteristics of concrete. Thus, it is important to correctly investigate the spatial distribution of insulation materials, and many researchers have studied the insulation/pore distribution and its effect on the material properties. Dorey et al. (2002) investigated the pore clustering effect on the material properties of ceramic. Won and Chau (2005) examined the concrete specimens with different constituent distributions. Chung et al. (2013) examined the correlation between the pore characteristics and the directional modulus of lightweight aggregates and evaluated the effect of the pore distribution on thermal properties of insulating specimens using micro-CT images Chung et al. (2016). Hao et al. (2016) investigated the effect of optimized porosity distribution of insulation materials by the variational method.

In general, the thermal conductivity decreases as the volume ratio of insulations increases, while the mechanical properties, such as strength and directional modulus, have a direct proportion to the insulation volume. In order to overcome the contrary behavior between these physical properties, several studies have been reported on related methods. Cabrillac and Malou (2000) proposed the modeling of anisotropic pores using a homogenization method, and Zake-Tiluga et al. (2014) investigated anisotropic behavior of compressive strength in porous ceramics. In particular, Cabrillac et al. (2006) suggested and examined concretes with anisotropic pores and their effect on the mechanical properties. Chung et al. (2016) also investigated the effect of ellipsoidal (anisotropic) pores on the thermal properties of materials using 3D printed samples. From these studies, it is demonstrated that a proper use of anisotropic pores can effectively overcome the contrary responses between thermal and mechanical properties without causing performance losses.

However, pores with anisotropic geometries are difficult to produce in a real specimen due to heterogeneity of concrete. Thus, rigid insulation materials with very low thermal conductivity can be used as artificial pores to examine the effect of anisotropic pores on the characteristics of insulating concrete. Several materials have been used as insulation materials; Gunduz (2008) used pumice aggregates as an insulation materials to investigate the effect on thermal properties and showed its effect in reducing the thermal conductivity, and Ng and Low (2010) investigated the thermal properties of specimens with newspaper sandwiched lightweight panels, which is much lower than that of conventional concrete. Jiang et al. (2013) adopted several natural leaves to improve the insulation of concrete by reducing energy consumption and environmental damage.

In this study, three different materials are utilized as insulation materials for the specimens: low-density expanded polystyrene (EPS), Af/Armaflex (Armacell, UK) made of elastomeric nitrile rubber, and corrugated paper used for packing box; these materials have very low thermal conductivity and can be utilized as alternative pores. To secure anisotropic pores (or insulations) in the sample, these three insulation materials were cut into a coin-shape, and a set of insulating mortar specimens with the coin-shaped insulations were generated to evaluate the effect of anisotropic pores on the material characteristics and properties. Using these artificial anisotropic insulations, the real samples with anisotropic pores can be produced, and their arrangements can be easily controlled. For characterization of the insulation distributions, probability functions, such as two-point correlation (Tewari et al. 2004; Gokhale et al. 2005) and lineal-path functions (Lu and Torquato 1992; Chung and Han 2010), were used. These probability functions were utilized to describe the degree of pore clustering and connectivity for a specific direction (Ke et al. 2009; Neithalath et al. 2010). Effects of anisotropic insulations on the material properties were examined experimentally and numerically.

The main objective of this study is to examine the effect of the spatial distribution of different anisotropic insulations on the physical properties of mortar specimens. For the purpose, different insulation materials were used to secure anisotropic artificial pores in the specimens. In addition, the effects of the insulation volumes and the spatial distribution of insulations on the insulating specimens were also investigated. For effective modeling of the specimens with anisotropic insulations, virtual insulating specimens with different distributions of insulations were generated, and their characteristics and properties were numerically computed. Then, a set of concrete (mortar) specimens with different insulations and arrangements were produced based on the numerical results. The insulation arrangements within the concrete specimens were confirmed using X-ray computed tomography (CT) without damaging the specimen. The material properties, such as the thermal conductivity, compressive strength, and Young’s modulus, were also evaluated from experimental methods. The thermal properties of the insulating specimens are examined using a Hot Disk, a device which satisfies ISO standard (22007-2) DeutscheNorm (2012). The compressive strength values of the specimens were measured using a Toni Technik loading tool DeutscheNorm (2010). The obtained properties were compared with those from simulations. The relationship between the probabilistic descriptions and the physical properties is investigated to evaluate the effect of anisotropic insulations on the material characteristics of insulating mortar specimens.

## 2 Concrete Specimens with Different Anisotropic Insulations

A set of virtual samples with different insulation distributions are designed to identify the effect of anisotropic insulations on the characteristics and properties of materials. Then, real mortar specimens with different insulation types and distributions are manufactured, and their properties as well as the spatial distribution of insulations are also investigated.

### 2.1 Modeling of Virtual Samples with Different Insulation Distributions

Figure 1 shows target virtual specimens with different numbers of anisotropic insulation layers. Each side of the virtual samples in Fig. 1 is discretized into 150 voxels for the *x*, *y*, and *z* directions, and each sample is composed of total of 3,375,000 voxels. All the coin-shape insulations have the same dimension with diameter of 0.16 and thickness of 0.032 in a unit cube with edge length 1, and each insulation layer in the *x*–*y* plane is composed of 25 anisotropic insulations (5 \(\times \) 5 in \( x{\times }y \) direction). The virtual specimens in Fig. 1 are denoted as L3 (Fig. 1a), L6 (Fig. 1b), and L9 (Fig. 1c) samples. Each specimen contains 3 (L3), 6 (L6), and 9 (L9) insulation layers with total of 75, 150, and 225 coin-shaped insulations, respectively. The volume ratios of anisotropic insulations in each specimen are 5.97\(\%\) (L3), 9.29\(\%\) (L6), and 13.27\(\%\) (L9). Using these samples, the effect of the anisotropic insulations with different spatial distributions can be examined numerically.

### 2.2 Preparation of the Mortar Specimens with Different Anisotropic Insulations

Physical properties of insulation materials.

Types | Mortar | EPS | Rubber | Paper |
---|---|---|---|---|

Thermal conductivity (W/m/K) | 1.835 | 0.029 | 0.033 | 0.050 |

Density (kg/m\(^3\)) | 1841 | 16 | 20 | 70 |

Specific heat (J/g/K) | 850 | 1300 | 1500 | 361 |

Elastic modulus (GPa) | 20 | 0.2 | 0.1 | 0.6 |

Poisson’s ratio | 0.2 | 0.3 | 0.42 | 0.05 |

Yield strength (MPa) | 80 | 0.1 | 0.2 | 0.4 |

Mix design for the mortar specimens in Fig. 2.

Specimens | Reference | EPS specimen | Rubber specimen | Paper specimen |
---|---|---|---|---|

Cement (g) | 750 | |||

Sand (g) | 1500 | |||

Water (g) | 375 | |||

W/C ratio | 0.5 | |||

EPS (layer) | – | 3/6/9 layers | – | – |

Rubber (layer) | – | – | 3/6/9 layers | – |

Paper (layer) | – | – | – | 3/6/9 layers |

## 3 Characterization and Property Measurements of Anisotropic Insulations

### 3.1 Probabilistic Characterization of Anisotropic Insulations

The insulation distributions in the specimens significantly affect the material properties of insulating concrete. For more detailed investigation of the spatial distribution of insulations, appropriate quantitative and qualitative methods are required. Here, low-order probability functions, such as two-point correlation and lineal-path functions, are used to examine the anisotropic insulation distribution, and their integrations are also utilized for the quantitative description.

#### 3.1.1 Two-Point Correlation Function

*i*denotes the insulation phase,

*r*is the distance between two points, \(\theta \) is the angle between a test line and the

*z*-axis, and \(\phi \) is the angle between the projection of a test line on the

*xy*-plane and the

*x*-axis. For two-phase materials that are classified into insulations and solids, the general limits of the two-point correlation function for the insulation phase are given as follows (Gokhale et al. 2005; Kumar et al. 2006):

*r*increases. \(P_{ii}\), can be calculated using a simple form of the function suggested by Gokhale et al. (2005) as:

*s*denotes the solid phase, \(f_s\) is the solid volume fraction, and \([P_L(\theta ,\phi )_{is}]\) is the number of intersections between a test line and the

*i*-

*s*phase interface per unit test line length.

*r*/

*D*, and

*D*is the specimen length. For the quantitative description of the insulation distributions, \(\overline{P_{ii}}\) values for different directions are calculated and assigned to each point of a grid represented on a sphere, which is composed of 1538 nodal points. Here, the 3D space is discretized into 1538 grids for effective visualization of anisotropy, and the calculation of \(\overline{r}\) is repeated for the whole discrete directions. The \(\overline{P_{ii}}\) values between the nodal points are calculated from the standard finite element interpolation, and detailed description of this method is shown in (Chung et al. 2013; Han and Dawson 2005).

#### 3.1.2 Lineal-Path Function

*r*is located in the insulation phase Chung et al. (2016). Unlike \(P_{ii}(r,\theta ,\phi )\), \(L_i(r,\theta ,\phi )\) can be utilized to examine the continuous connectivity of the insulation phase for a specific direction because the function only includes the case that a whole line is positioned in the insulation phase Lu and Torquato (1992); therefore, \(L_i(r,\theta ,\phi )\) can be utilized as a complementary function of \(P_{ii}(r,\theta ,\phi )\). The general limits of \(L_i(r,\theta ,\phi )\) are given as:

### 3.2 Investigation of the Physical Properties of the Specimens

The thermal and mechanical properties of the specimens with different insulations and distributions are examined using numerical as well as experimental methods. The material responses of the virtual samples are evaluated to investigate the anisotropy of the properties using finite element (FE) analysis. In addition, the thermal conductivity and compressive strength values of the specimens with different types of insulations are examined using experimental tools.

#### 3.2.1 Numerical Simulation for Thermal and Mechanical Analysis

To investigate the anisotropic effect on the material properties, the thermal and mechanical responses of the virtual samples in Fig. 1 are evaluated using FE simulations. The ABAQUS package ABAQUS (2013) is used for the numerical simulations, and detailed descriptions on the FE formulations for thermal and mechanical analysis are in (Chung et al. 2016; Incropera et al. 2006); only a brief description is presented here.

*C*is the specific heat (J/g/K), and

*k*is the thermal conductivity (W/m/K).

*T*is the temperature (K), \(T^{*}\) is the surrounding temperature (K), \(\lambda \) is the heat loss coefficient (1/s), and

*t*is the time (s).

*n*is the directional component, and

*L*is the characteristic length.

The required input parameters for the heat analysis, such as the bulk thermal conductivity and specific heat of hydrated mortar and insulation materials, are obtained from experiments using a Hot Disk device that satisfies ISO standard (22007-2) DeutscheNorm (2012); the parameters used here are presented in Table 1. For the boundary condition, a constant temperature (60 \(^{\circ }\)C) is imposed on the top side of the specimen, while heat loss is allowed only in the opposite side along in each direction. The remaining surfaces are considered to have no heat loss, and the surrounding temperature is set as 22 \(^{\circ }\)C. Heat loss coefficient, \(\lambda \), is obtained from the Hot Disk device and selected as 1.6 (1/s). In this study, the thermal conductivities for all the specimens are measured in the *x* and *z* directions to examine anisotropic thermal properties.

*d*is the scalar stiffness degradation variable between 0 (undamaged material) to 1 (fully damaged material), \(\varvec{D}_{0}^{el}\) is the initial elastic modulus, \(\varvec{D}_{0}\) is the degraded elastic stiffness, \({\varvec{\epsilon }}\) is the total strain tensor, and \({\varvec{\epsilon }^{pl}}\) is the plastic strain tensor.

Each elemental stress is calculated at the center of each element, and the effective stress is obtained from the element stresses by integrating over the whole volume. For the boundary condition, a displacement boundary condition is imposed on the top surface in each *x* and *z* direction, while a fixed boundary condition is applied to the bottom plane. Other remaining lateral surfaces are set to be traction free. The parameters for the CDP model, such as dilation angle and eccentricity, are selected and adjusted from the data in (Kmiecik and Kaminski 2011; Jankowiak and Lodygowski 2008). The input parameters for the mechanical simulations of the specimens with different insulations are listed in Table 1. The simulation results are compared with experiments for validation purpose. The effect of different insulations and the correlation between the insulation distribution and the directional compressive strength are also confirmed from the results

#### 3.2.2 Experiments for the Evaluation of Material Properties

Using the Hot Disk machine (Hot Disk AB, Sweden), thermal properties, such as thermal conductivity, thermal diffusivity, and specific heat capacity can be effectively measured, and the obtained results are utilized for the numerical simulations as the input parameters. This device is based on the use of a transiently heated plane sensor, and the sensor is sandwiched between two sheets of an insulating material to be measured. Detailed description of the measurement process is shown in Fig. 3a. The compressive strength of the specimens are also evaluated using the Toni Technik (Zwick Roell, Germany) machine in Fig. 3b, a device which meets German standard 12390-4 DeutscheNorm (2010) with loading rate of 0.50 MPa/s and with loading capacity of 3000 kN. Likewise the thermal property, the strengths of the specimens are evaluated for the different (*x* and *z*) directions to confirm the effect of anisotropic insulations on the mechanical properties of the specimens. All tests have been carried out on three specimens and the mean value is considered in each case. Here, at least three specimens of each case are tested to enhance the accuracy, and only the mean values are presented.

## 4 Characteristics and Properties of the Insulating Specimens with Different Anisotropic Insulations

The characteristics of the insulation distributions are described using the methods in Sect. 3.1 In particular, the anisotropic characteristics of the specimens with different insulation distributions are identified, and their effects on the material properties are examined using the numerical and experimental methods.

### 4.1 Anisotropic Characteristics of the Virtual Insulating Specimens

*x*,

*y*, and

*z*directions; Fig. 4a–c are the two-point correlation function (\(P_{ii}(r)\)), and Fig. 4d–f are the lineal-path function (\(L_i(r)\)). In each function,

*r*represents the distance between two random points, and

*D*is the specimen edge length. In these figures, the porosities and the directional characteristics of the insulation distributions are clearly described; the porosities in each function are 0.0597, 0.0929, and 0.1327 for L3, L6, and L9 samples, respectively. \(P_{ii}(r)\) and \(L_i(r)\) in Fig. 4 show almost the same functions in the

*x*and

*y*directions, while the function values in the

*z*direction are smaller than other directions; this represents that the size of the insulations in the

*z*-direction is smaller than that of other directions, and the insulation distributions in the specimens are anisotropic. In Fig. 4a–c, the relative degree of clustering of insulations can be estimated using \(P_{ii}(r)\). In particular, \(L_i(r)\) can be used to demonstrate the anisotropy of the coin-shaped insulation used in this study. The ratio between the diameter and the thickness of each coin-shaped insulation is designed as approximately 5:1. In Fig. 4d–f, the function values in the

*x*and

*y*directions are zero when

*r*/

*D*reaches 0.16, while the function for the

*z*-direction is zero when

*r*/

*D*is about 0.3; this ratio is almost identical with that of the coin-shaped insulation, and it is examined that the probability functions used here can be effectively used to describe the directional characteristics of insulation materials.

For the quantitative description of the insulation distribution, \(\overline{P_{ii}}\) of the specimens in Fig. 1 is also investigated. To describe the relative anisotropy of the insulation distribution, \(\overline{P_{ii}}\) for every direction is divided by the minimum value of \(\overline{P_{ii}}\) for each specimen, and the \(\overline{P_{ii}}\) values are visualized on a sphere mesh, as shown in Fig. 5. In these figures, the indexed values (\(\overline{P_{ii}}\)/min\( \overline{P_{ii}}\)) for the *x*–*y* plane is distinctly larger than that of the *z*-direction. The maximum anisotropy ratio of \(\overline{P_{ii}}\) between different directions decreases as the number of insulation layers for the *z*-direction increases: 2.11 (L3), 1.81 (L6), and 1.62 (L9). In addition, the anisotropy ratio of the integration of \(L_i(r)\), \(\overline{L_{i}}\), bears the same characteristics, as 4.5 (L3), 4.2 (L6), and 3.3 (L9), although they are not visualized here. The maximum anisotropy ratio decreases as the total volume of the insulations increases because the insulation layers are stacked only in the *z*-direction. These results demonstrate that \(\overline{P_{ii}}\) as well as \(\overline{L_{i}}\) can be efficiently utilized to describe the characteristics of the insulation distributions, and the insulation distributions in each specimen are anisotropic.

### 4.2 Material Responses of the Virtual Insulating Specimens

*x*-direction, the direction parallel to the flat surface of the coin-shaped insulation; however, the less heat flows through the

*z*-direction than other (

*x*and

*y*) directions because the flat surfaces of the coin-shaped insulations disrupt the heat flow. In all directions, the solid region where heat transfers mostly, decreases as the volume of insulations increases; therefore, the total amount of heat which flows through the solids decreases as more coin-shaped insulations are contained in the specimen. The effect of the coin-shaped insulations can be also identified from the temperature isosurfaces in Fig. 6b, d, and f. In the isosurfaces for the

*x*-direction, the isosurfaces are almost flat because the insulations parallel to the heat flow direction rarely affect the heat transfer. However, in the right figures of Fig. 6b, d, and f, the fluctuations of the temperature isosurfaces can be found near the insulations; this result demonstrates that the coin-shaped insulation strongly affects the hear flow for the perpendicular direction to its flat surface. The same trends are also examined for the use of different insulations, such as EPS and Paper.

*x*-direction), although the vicinity of the insulations shows less stress values than other parts. In contrast, when the loading is applied to the

*z*-direction, perpendicular to the flat surface of the anisotropic insulation, the stress concentrations can be found near the edge and vertex of the coin-shaped insulations, and these stress concentrations can be critical for early specimen failure from that location; it denotes that the direction of coin-shaped (anisotropic) insulations affects the mechanical responses of the specimen significantly. Likewise the thermal responses, the same tendencies of the stress distribution are confirmed for the different insulation materials.

For the quantitative investigation of the material responses, thermal conductivity and compressive strength are calculated from the simulation results in Figs. 6 and 7, as shown in Fig. 8. In Fig. 8a, the thermal conductivities of the virtual specimens with different insulation distributions are presented. For all insulation materials, the thermal conductivity as well as compressive strength decrease as the number of insulation layers increases. In particular, both material properties in the *z*-direction significantly decrease more than those of the *x*-direction as the layer number increases. From these results, as shown in Figs. 6 and 8, it is confirmed that the material properties are more affected by the coin-shaped insulations in the perpendicular direction to the flat surface of the insulation. The effect of the different insulations can also be examined from the graphs; the use of different insulations rarely affects the thermal and mechanical properties for the *x*-direction, as shown in Fig. 8. Otherwise, the material properties for the *z*-direction are affected by the type of insulation, especially the compressive strength of the specimen. In these results, it is shown that the EPS is the most effective to reduce the thermal conductivity because of its higher specific heat Owrak et al. (2015), while corrugated paper is the most beneficial insulation material for larger strength of the specimen because of its larger elasticity and strength. Fig. 8 is the theoretical result to investigate the effect of different insulations and distributions on material characteristics and properties.

### 4.3 Physical Properties of the Insulating Specimens with Different Anisotropic Insulations

## 5 Conclusions

The anisotropic insulation and its effect on the material characteristics are examined. To secure anisotropic insulations in the specimen, a set of coin-shaped insulations with different materials, such as expanded polystyrene (EPS), elastomeric nitrile rubber (Rubber), and corrugated paper (Paper), are prepared, and these insulations are used to produce mortar specimens with different arrangements. The virtual specimens are designed to evaluated the effect of anisotropic insulations on the material using numerical methods, and the results are adopted to produce real insulating specimens. Low-order probabilistic functions and their modified indexes are utilized for the characterization of the insulation distribution. The physical properties, such as thermal conductivity and compressive strength, are examined using both FE simulations and experimental tools. Then, the correlation between the material characteristics and properties is investigated.

The anisotropy of the insulation distribution is effectively examined using the characterization methods utilized here. Comparing the directional material properties, it is demonstrated that the thermal conductivity is smaller when heat flows in the direction perpendicular to the flat surface of the coin-shaped insulation, while the strength is larger when the loading direction is parallel to the flat surface. Among the three insulation materials used here, EPS is the most effective material to improve the insulation effect, although strength loss should be carefully considered. The results confirm that appropriately arranged anisotropic insulations can be effectively used to obtain a material with low thermal conductivity by minimizing strength loss, and anisotropic insulations/pores can be a promising method for better insulating material without increasing the insulation/pore volume.

## Declarations

### Acknowledgements

The project is supported by the German Federal Ministry of Education and Research (BMBF, Project Number: 13XP5010B and 01DR16007) and the German Academic Exchange Service (DAAD, Ref. No.: 91563255). The authors also want to thank Mr. Paul H. Kamm (Helmholtz Centre Berlin) for his assistance in CT imaging.

**Open Access**This article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made.

## Authors’ Affiliations

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