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Realistic Evaluation of Reinforcement Bond Strength in Alkali-Activated Slag Concrete Exposed to Elevated Temperature

Abstract

Alkali-activated concrete (AAC) has attained great popularity since finding it as an alternative to Portland cement concrete due to its superior characteristics in terms of mechanical properties and durability, and its low negative environmental impact. This research investigated both experimentally and analytically the bond behavior between alkali-activated slag concrete (AASC) and steel rebars considering some important parameters (rebar diameter and development length-to-diameter ratio) before and after exposure to elevated temperature using beam-end bond testing technique. The obtained experimental results were compared with those obtained from applying the CEB-FIP model and the well-known available equations in the literature. A modified model was proposed for predicting the bond behavior of AASC. Results have showed that the CEB-FIP model provides more conservative values for bond strength compared to the experimentally obtained results which increases the safety level when estimating the bond strength for design purposes. The proposed modified model achieved a higher correlation with the experimental results than the CEB-FIP model at ambient temperature.

1 Introduction

The environmental impact of ordinary Portland cement (OPC) production is mainly due to the energy consumed intensively in its manufacturing process. Moreover, the cement industry alone is responsible for approximately 6–7% of the total greenhouse gases emitted all over the world (Bijen, 1996; Pal, 2018; Refaat et al., 2021). To suppress these drawbacks, the construction industry is looking forward to develop innovative binders valid to be an alternative to OPC (Bastidas et al., 2008; Gong & Yang, 2000; Grutzeck et al., 2004; Khalil et al., 2020; Kotop et al., 2021; Palomo et al., 1999; Provis & Van Deventer, 2009a; Puertas et al., 2000). To that extent, the ecological dream of producing Portland cement-free concrete, started to come true, when researchers began to utilize industrial by-products or natural materials that are rich with aluminate and silicate, and activating them by alkali-activators. The obtained alkali-activated binders get mixed with both of fine and coarse aggregates and when being hardened through appropriate conditions forming alkali-activated concrete (AAC) (Amer et al., 2020, 2021a, 2021b; Davidovits, 1991; Lee & Lee, 2013; Ravikumar et al., 2010; Thomas & Peethamparan, 2015; Zhang et al., 2020). CO2 emissions result from manufacturing alkali-activated binder is around 50–80% lower than OPC composites production (Duxson et al., 2007; Provis & Van Deventer, 2009b).

Many significant studies have been conducted on AAC to address the manufacturing of AAC using different types of source materials for obtaining desirable mechanical characteristics (Abdulrahman et al., 2021; Allaoui et al., 2022; Okoye et al., 2015; Xie et al., 2018), while studies concerned with its structural performance are still limited (Ma et al., 2018; Mo et al., 2016; Nikbakht et al., 2021; Unis Ahmed, et al., 2022). The bond behavior of steel-reinforced AAC is a vital property that has to be established to ensure the achievement of sufficient bond between the steel rebars and the surrounding AAC (Al-Azzawi et al., 2018; Albidah et al., 2020; Romanazzi et al., 2022; Yang, et al., 2022). Particular investigation has been performed to evaluate the bond performance between AAC and rebars (Ahmad & Bhargava, 2020; Alharbi et al., 2021a; Sarker, 2011; Sofi et al., 2007; Zhang et al., 2016). It was drawn that AAC demonstrated better bond performance compared with conventional concrete (Castel & Foster, 2015; Sarker, 2011). Also it was reported that the bond performance was improved with increasing both of the concrete cover thickness, compressive strength, and the ratio between thickness of concrete cover and diameter of rebars (Sarker, 2011). Several parameters affecting the bond performance such as compressive strength, concrete cover, rebars characteristics (mainly diameter and surface texture), confinement conditions and the bond stress–slip relationship were studied (Zhang et al., 2016). Most of studies are primarily related to investigate the bond behavior in ambient temperature. Insufficient attention has been directed towards the bond performance between AAC and rebars at high temperature (Chen et al., 2018).

Reinforcement bar bond characteristics in concrete exposed to elevated temperatures are crucial for maintaining structural integrity in case of fire. A well-established research works investigated the bond characteristics between the reinforcement bars and OPC concrete (Alharbi et al., 2021b). Some recent studies (Morley & Royles, 1980; Yin et al., 2011) revealed that the strength of concrete reduced as the temperature increased; at elevated temperature, the degradation of concrete–rebar bond strength was significant.

H.Y. Zhang et al. investigated the bond behavior of metakaolin–fly ash based AAC with different-diameter rebars, using pull-out tests, after exposure to elevated temperatures up to 700 °C. It was shown that the AAC did not demonstrate significant deterioration in bond strength except when exposed to elevated temperature above 300 °C. Also, AAC showed similar or better bond characteristics than OPC concrete with similar compressive strength (Zhang et al., 2018). Jiang et al. performed a laboratory study to investigate the steel rebar-to-paste bond behavior for both AAC and OPC concrete after exposing to very high temperatures (up to 1200 °C). This study revealed that AAC retained some residual bond strength even after exposing to 1200 °C, While OPC concrete completely disintegrated at 800 °C, which indicated to the excellent bonding performance of AAC at the extreme temperatures (Jiang et al., 2020). Ramagiri et al. reported that increasing the slag content in the blended binder (fly ash + slag) of AAC increased the bond strength of AAC at a constant activator modulus. Also, it was reported that the AAC mix that contains 30% slag in the blended binder exhibited a superior high-temperature performance in terms of residual compressive and bond strength (Ramagiri & De Maeijer, 2022). Paswan et al. investigated the bond behavior at elevated temperature up to 800 °C between rebars and fly ash–slag based AAC as a function of compressive strength, rebar diameter, embedment length and concrete cover by considering the obtained ultimate bond stress, slip, and load at failure compared with those of control cement concrete. It was concluded that the bond performance of AAC was effective compared with that of the cement concrete. Also, it was reported that the bond strength of AAC exposed to elevated temperatures increased with an increase of temperature up to 400 °C, due to the curing of low-calcium fly ash, and then decreased. The decrease in bond strength was about 69% at 800 °C (Paswan et al., 2020).

Many researches proved the superiority of AAC in the mechanical properties and durability compared with the conventional concrete. However, limited studies have been investigated the bond performance between AAC and steel rebars, and most of them were conducted using the well-known pull-out test on lollipop specimens because of its simplicity, while rare studies have used the beam-end specimens which are more realistic and accurate, because of the relative difficulty of its test setup. Moreover, researches investigating the bond behavior of AAC after exposure to elevated temperatures are still limited especially for those that used slag only as a binder. So, this paper concerned with investigating the bond behavior between AASC, using binder totally from slag, and steel rebars considering the rebar diameter and development length-to-diameter ratio using the beam-end technique, which is consider the most effective technique, at both ambient and elevated temperatures.

2 Experimental Program

2.1 Materials

GGBFS was used as the binder in this study. The chemical composition of GGBFS is presented in Table 1. The coarse aggregate was natural crushed limestone with nominal maximum size of 10 mm, and the fine aggregate (natural sand) was with fineness modulus of 2.77. The alkaline activator was a mixture solution of sodium silicate and sodium hydroxide. The solution of sodium hydroxide solution was prepared by dissolving flakes of pure sodium hydroxide in potable water, while the sodium silicate solution was obtained from a local supplier. The used sodium hydroxide flakes had a chemical composition of 60.25% Na2O and 39.75% H2O, while the chemical composition of the used sodium silicate solution was 31.00% SiO2, 11.98% Na2O, and 57.00% H2O. The rebars used to investigate the bond behavior were steel ribbed bars with properties as shown in Table 2. The mix proportions for the used AASC and its characteristics are shown in Table 3.

Table 1 Chemical compositions of GGBFS (mass %)
Table 2 Characteristics of used steel rebars
Table 3 Mix proportions and properties of the used AASC

2.2 Test Specimens

Nine beam-end specimens with of 200 mm in wide, 300 mm in height, and 600 mm in length were investigated. Both of tension and compression reinforcement was two deformed rebars with diameter of 12 mm positioned in the beam corners, while the shear reinforcement was stirrups with 8 mm in diameter with spacing of 125 mm. The configuration of test specimen was determined to fulfill the requirements of the ASTM A 944 (2005). Fig. 1 illustrates the configuration and presents the dimensions of the used specimens. One tested steel rebar was placed in the tension side for each test specimen; the bottom concrete cover of the tested rebar was 50 mm, while the side concrete cover was 100 mm, and these covers were kept constants for all tested specimens. A plastic tube was used to make the first 50 mm distance from the tested rebar, measured from the loaded end concrete surface, debonded. This distance is called the lead length which should be achieved to avoid the possible conical failure. The tested bonded length, which calculated according to the investigated bond length to diameter (L/d) ratio, followed the lead length (50 mm distance), and then the remaining part of the tested rebar was debonded using also plastic tube as shown in Fig. 1.

Fig. 1
figure 1

Configuration and dimensions of beam-end test specimen

2.3 Preparation and Testing of Specimens

Mixing criteria implemented in this work for the alkali-activated concrete initiated with mixing the dry materials, GGBFS and aggregates, in the pan of mixer for about 1 min. Then, the alkaline activator was added to the dry mixture and then mixing for around 4 min until the mixture became homogeneous. The preparation process of the alkaline activator was by mixing the sodium hydroxide flakes, sodium silicate solution and potable water for around 1 h before adding it to the dry mixture until its average temperature was about 30 °C. Before casting, the cage of reinforcement bars was positioned in the mold and then the tested steel rebar oriented horizontally in its proper position as presented in Fig. 2. Plastic tubes and sticky tape were used to make the bond breakers for the tested rebars to achieve the required bonded length for testing as illustrated in Fig. 3. The test specimens were demolded after 24 h from casting, and then kept in the laboratory at the ambient temperature (25 ± 2 °C) and relative humidity (50 ± 5%) until the testing date.

Fig. 2
figure 2

Shape of reinforcement cage and tested rebar in the mold

Fig. 3
figure 3

Shape of tested rebars before placing in the mold

For the specimens that were exposed to elevated temperatures, their apparent parts of their tested rebars were painted with an anti-rust material to keep it from being corroded by elevated temperatures. After painting the rebars, they were covered with a heat-insulation material (ceramic fiber fabrics) to prevent the rapid transfer of heat to the embedded part of rebars inside the concrete and also so that its tensile strength would not be affected by the elevated temperatures. Fig. 4 shows the beam-end specimens after preparing the rebars.

Fig. 4
figure 4

Preparation of beam-end specimens before exposure to the elevated temperature

The configuration of the test setup of specimens is illustrated in Figs. 5 and 6. The reaction steel plate was positioned at the specimen bottom (compression side) to achieve uniform distribution for the induced stresses. The applied tension force acting on the tested steel rebar generated by using a hydraulic jack with capacity of 300 kN. The test specimen was fixed in its position by anchoring it to the reaction steel frame using two steel plates with four steel threaded bars and nuts. The values of applied tension loads were measured by using a special load cell positioned between the hydraulic jack and test specimen which connected to specimen by a threaded part in the outer part of the tested rebar and connected to the hydraulic jack using an external threaded bar. Slippage that occurred in the free end of the tested steel rebar was recorded by using LDVT.

Fig. 5
figure 5

Schematic for the beam-end specimen test setup

Fig. 6
figure 6

Setup of beam-end specimen test

The bond strength, \(\tau_{u}\), was determined based on the obtained ultimate load, \(P_{u}\), resisted by the tested steel rebar by using Eq. (1) (Castel & Foster, 2015):

$$\tau_{u} = \frac{P_{u} }{\pi \cdot \emptyset \cdot L},$$
(1)

where τu = bond strength (MPa); Ø = diameter of tested rebar (mm); L = bonded length of tested rebar (mm); Pu = ultimate load resisted by the tested rebar (pull-out) (N).

The axial tensile stress, \(\sigma_{u}\), in the tested rebar corresponding to its ultimate bond strength, was determined by using Eq. (2):

$$\sigma_{u} = \frac{{P_{u} }}{{\pi . \emptyset ^{2} /4}},$$
(2)

where \(\sigma_{u}\) = tensile stress in the tested rebar (MPa); Ø = diameter of tested rebar (mm); Pu = ultimate load resisted by the tested rebar (pull-out) (N).

2.4 Test Matrix

In this study, pulling-out testing was performed on beam-end specimens to investigate the bond behavior. The beam-end technique was selected because of its simulation to the actual bond between the rebars and concrete in the reinforced concrete elements that subjected to flexure (Shamseldein et al., 2018).

Taguchi method was applied to design the experiments to reduce the number of tested beams while preserving the possibility of interpreting and analyzing the test results for the studied different factors and levels. Three factors related to bond behavior with three levels for each factor were considered. Table 4 presents the parameters and levels that employed in the Taguchi method. By using Taguchi design and according to L9 array, nine beams were obtained as shown in Table 5.

Table 4 Parameters and levels employed in Taguchi design
Table 5 Test matrix

The code of specimens presented in Table 5 refers to the studied parameters. The first part describes the rebar diameter, the second part describes the exposure condition, and the last part describes the development length-to-diameter ratio. For example, specimen (D12-T300-6) refers to a specimen reinforced by 12-mm-diameter rebar, exposed to elevated temperature of 300 °C, and the applied development length-to-diameter ratio is 6.

2.5 Heating Regime

After 28 days of curing, the prepared test specimens were exposed to elevated temperatures in an electric furnace with a temperature capacity of 1200 °C as shown in Fig. 7. Six specimens were exposed to two degrees of temperature (300 and 600 °C), three specimens for each temperature degree. The heating rate of the furnace was 5 °C/min. After reaching the required temperature, the heated specimens kept at this temperature in the furnace for a period of 1.5 h to achieve the temperature homogenization in the specimens. Then, the heated specimens were cooled naturally by opening the ventilation hole in the furnace to ambient temperature. Fig. 8 presents the time–temperature regime of all targeted elevated temperatures that applied on the test specimens.

Fig. 7
figure 7

The used electric furnace

Fig. 8
figure 8

Applied time–temperature regime

3 Results and Discussion

To determine the concrete compressive strength of the tested beams, core specimens were extracted from the beams after testing from a location far from the failure positions, using a core cutter device as shown in Fig. 9. Table 6 presents the test results for the compressive strength of tested specimens before and after exposing to the elevated temperatures. Moreover, Table 7 shows the results of all test specimens. Ultimate bond strength, \(\tau_{u}\), free-end slippage that is corresponding to the obtained ultimate bond stress, Su, maximum tension stress induced in the tested steel rebar that is corresponding to the ultimate bond strength, \(\sigma_{u}\), as a percentage of the maximum tensile strength of the tested steel rebar, fu, the ascending branch slope, Ka = \(\tau_{u}\)/Su, and the observed modes of failure are summarized in Table 7.

Fig. 9
figure 9

Extracting cylindrical specimens and testing them in compression

Table 6 Test results of compressive strength
Table 7 Test results of beam-end specimens

3.1 Elevated Temperatures Damage

The damage caused by applying the elevated temperatures were evaluated for all heated test specimens by performing the unit weight, compressive strength and ultrasonic-pulse velocity tests on specimens extracted from the beams after testing. Table 8 presents the results of all carried-out tests. Percentage of unit weight loss, compressive strength loss and ultrasonic-pulse velocity loss were calculated and plotted as presented in Fig. 10. Also, the heated specimens were inspected visually after removing them from the furnace, where tiny cracks scattered on the surface with slight thermal spalling for the specimens’ edges were observed in all heated specimens.

Table 8 Tests results for the evaluation of beam-end specimens
Fig. 10
figure 10

Percentage of unit weight loss, compressive strength loss and ultrasonic-pulse velocity loss for all extracted specimens

3.2 Mode of Failure and Cracking Pattern

Cracking patterns resulting at failure for all test specimens are presented in Fig. 11. The failure mode of all beams was splitting mode failure, where a single crack started at the loaded end of specimen and propagated in the longitudinal direction of the tested rebar towards the specimen free end, then this longitudinal single crack was branched out into two cracks towards the edges of the tested specimen at the end of the bonded length of the tested rebar. It can be said that a typical cracking pattern and failure mode were obtained for the tested specimens are as illustrated in Fig. 12. The obtained crack pattern was similar to that of OPC concrete under pull-out load which agreed with what found by Sarker (2011). There was no significant difference observed in the obtained cracking pattern and failure mode due to the elevated temperature exposure. This can be attributed to the high stability, which means no significant changes occurred, of the AAC products, which are generated due to the hydration and polymerization of its binder, in the presence of alkaline activator, at elevated temperatures. Also, the obtained porous micro-structure in AAC makes it have better performance at elevated temperatures (Jiang et al., 2020).

Fig. 11
figure 11

Modes of failure and cracking patterns for all tested beam-end specimens

Fig. 12
figure 12

Typical cracking pattern of the tested beam-end specimens

3.3 Bond Stress–Slip Relationships

Fig. 13 presents the relationships between bond stress and slippage that occurred at the free end of all tested specimens. These relationships were separated into three groups as illustrated in Figs. 14, 15 and 16 according to the rebar diameter to clarify the relationships and the differences between them. The bond stress–free-end slip relationships of “D12-T25-4”, “D12-T300-6” and “D12-T600-8” specimens are presented in Fig. 14, while the bond stress–free-end slip relationships for “D16-T25-8”, “D16-T300-4” and “D16-T600-6” specimens are presented in Fig. 15, and the bond stress–free-end slip relationships for “D22-T25-6”, “D22-T300-8” and “D22-T600-4” specimens are presented in Fig. 16.

Fig. 13
figure 13

Bond stress–slip relationships of all test specimens

Fig. 14
figure 14

Bond stress–slip relationships of the case of 12-mm-diameter rebars

Fig. 15
figure 15

Bond stress–slip relationships of the case of 16-mm-diameter rebars

Fig. 16
figure 16

Bond stress–slip relationships of the case of 22-mm-diameter rebars

As shown in Table 7 and Figs. 14, 15 and 16, the bond stress–slip relationships of the specimens that were exposed to 25 °C (ambient temperature) demonstrated a steep ascending branch at the low values of slippage, then followed by a soft increasing up to the maximum bond stress. These specimens had achieved the highest values for the ascending branch slope. For the specimens exposed to elevated temperatures, their bond stress–slip relationships showed less steep ascending branches up to the maximum bond stress than those of specimens at ambient temperature. This result is clearer from the values of ascending branch slopes reported in Table 7. It can be seen that by increasing the temperature degree of exposure, the value of ascending branch slope was decreased. Also, it was noticed that the exposure to elevated temperatures caused a significant reduction in the maximum bond stress, and an increase in the free-end slippage that was corresponding to the maximum bond stress. Moreover, test specimens that were exposed to elevated temperatures achieved the lowest slopes for the ascending branch.

To surmount the difficulty of investigating how the different parameters affect the values of τu and Su, program of Minitab was employed to determine the signal-to-noise (S/N) ratio for all considered parameters affect both of τu and Su as shown in Figs. 17 and 18, respectively. Also, ANOVA approach was used by employing the program of Qualitek-4 to calculate the percentage of participation and optimum level of all considered parameters on both of τu and Su as given in Tables 9 and 10, respectively.

Fig. 17
figure 17

The significance of main parameters affecting “τu” (Minitab program)

Fig. 18
figure 18

The significance of main parameters affecting “Su” (Minitab program)

Table 9 Percentage of participation and optimum level for all considered parameters on τu
Table 10 Percentage of participation and optimum level for all considered parameters on Su

It can be observed from Fig. 17 and Table 9 that the exposure temperature was the most significant parameter that affects the value of “τu. The participation percentage was 83.27% and the optimum level was 25 °C. This means that by increasing the exposure temperature, the maximum bond stress was decreased, which can be attributed to the obtained decrease in the compressive strength and tensile strength after exposing to the elevated temperatures. The degradation in τu when exposing to elevated temperature above 300 °C was more significant. The reduction in S/N ratio at temperatures of 300 °C and 600 °C from the ambient temperature of 25 °C was 8.32% and 20.40%, respectively. This is agreed with what reported by H.Y. Zhang et al. (2018) (Zhang et al., 2018).

The bar diameter is the second significant parameter with a participation percentage of 10.76% and the 12 mm bar diameter (the lowest diameter) was the optimum level, as presented in Table 9. This demonstrates that the bond behavior of small-diameter rebars was better than that of large-diameter rebars as shown in Fig. 17. The improvement in the bond behavior occurred due to more favorable ratio between bond surface area and cross-sectional area of rebars (Bamonte et al., 2004; Wu & Zhao, 2013).

The L/d ratio was achieved the lowest value for the percentage of participation, 4.65%, with optimum level of 8. This indicates that by increasing the L/d ratio, the τu was increased as shown in Fig. 17. The increase of τu due to increasing the L/d ratio was not significant. The increase in S/N ratio for L/d of 6 was 4.80% higher than that for L/d of 4, while the increase in S/N ratio for L/d of 8 was 6.76% higher than that for L/d of 4. This indicates that increasing the L/d ratio does not increase τu significantly which agreed with what found by Eligehausen et al., (1982), Xu (1990) and Harajli et al., (2004).

From Fig. 18, it can be observed that the Su decreased by increasing of both rebar diameter and exposure temperature and increased by increasing of the L/d ratio. As reported in Table 10, the most significant factor on Su was the exposure temperature, then rebar diameter and finally the L/d ratio with percentages of participations of 82.81%, 10.74% and 4.85%, and with optimum levels of 25 °C, 12 mm and 8, respectively.

4 Analytical Study

4.1 Available Models

There is a need to verify the bond behavior of AASC using the available bond models used for OPC concrete to see how accurate these models predict the bond behavior of AASC. Two common models were utilized to predict the bond behavior for the conventional concrete with rebars were used in this analytical study. The first one was in the CEB-FIP model (Comite EURO—International du Beton, 1990) while the second one was the model that proposed by Maree 2014 (Farghal Maree & Hilal Riad, 2014). These two models were used to compare the experimental results of bond behavior with those obtained analytically from the aforementioned two models.

In CEB-FIP, the relationship between bond stress and slippage is defined by a set of equations, which are based on several parameters: concrete compressive strength, rebar diameter, type of reinforcement (smooth or deformed), confinement conditions and bond conditions. The analytical relationship of bond stress–slip in accordance with CEB-FIP model is presented in Fig. 19.

Fig. 19
figure 19

Bond stress–slip relationship (CEB-FIP model) (Comite EURO—International du Beton, 1990)

In Fig. 19, the first branch, ascending, which is a non-linear part, represents the phase in which the ribs, on the surface of rebars, penetrate and interlock through the mortar matrix of concrete, characterized by microcracking and crushing locally. Maximum slip of this first branch (ascending) is considered the characteristic slip which denoted as S1. The constant horizontal part, which occurs in case of confined concrete only, is referring to the shearing and advanced crushing of concrete between the ribs of rebar. The maximum slip of this part is denoted as S2. This constant part is followed by descending branch which is referring to the decrease in the bond resistance because of the induced cracks occurred in the longitudinal direction of rebars due to splitting. The maximum slip of this descending branch is denoted as S3. The lower horizontal part refers to the residue of bond strength, which is retained due to minimal transverse reinforcement, while maintaining a particular integrity intact degree.

For monotonic loading, bond stress between concrete and rebar can be determined as a function of the relative displacement, S, according to Eqs. (3) to (6). The values of parameters in these equations are defined in Table 11:

$$\tau = \tau_{{{\text{max}}}} \left( {\frac{S}{{S_{1} }}} \right)^{\alpha } ,\,\,\, 0 \le S \le S_{1} ,$$
(3)
$$\tau = \tau_{{{\text{max}}}} ,\,\,\, S_{1} < S \le S_{2} ,$$
(4)
$$\tau = \tau_{{{\text{max}}}} - \left( {\tau_{{{\text{max}}}} - \tau_{f} } \right)\left[ {\frac{{S - S_{2} }}{{S_{3} - S_{2} }}} \right], \,\,\,\,S_{2} < S \le S_{3} ,$$
(5)
$$\tau = \tau_{f} , \,\,\,S_{3} < S.$$
(6)
Table 11 Defining parameters of the bond stress–slippage relationship

Maree 2014 investigated the bond characteristics for two types of conventional concrete (Normal Weight Concrete “NWC” and Light Weight Concrete “LWC”) with steel rebars using pull-out test for both beam-end and lollipop specimens. This study investigated the bond of straight, deformed, and unanchored steel rebars with LWC in flexural elements with investigating the validity of both available design codes and bond models to predict the bond behavior for LWC. The main parameters considered in this study were concrete type (NWC and LWC), diameter of rebars (12, 16 and 22 mm) and bonded length-to-diameter ratio (2, 3 and 4).

At the end of this study, Maree proposed modifications in the main parameters of the CEB-FIP model to consider the effect of both concrete type and bar diameter on the bond stress–slippage relationship. These modifications were in characteristic slippages (\(S_{1}\)) and (\(S_{2} )\) and bond strength (\(\tau_{{{\text{max}}}}\)) as presented in Table 11.

4.2 Comparative Study

Comparison between the two aforementioned models with the obtained experimental results was conducted. The results of this comparison are presented in Figs. 20, 21 and 22. It was observed that the CEB-FIP model demonstrated underestimated values for the bond strength and revealed bond–slip relationships with steeper descending branches than experimental results at both ambient and elevated temperature. However, it was observed that the value of bond strength obtained from CEB-FIP model approached the experimental results with increasing the exposure temperature. The model proposed by Maree 2014 gave over-estimated values for the bond strength and gave bond–slip relationships with steeper descending branches than the obtained experimental results at ambient and elevated temperature.

Fig. 20
figure 20

Analytical versus experimental bond–slip curves (specimens of 12-mm-diameter rebars)

Fig. 21
figure 21

Analytical versus experimental bond–slip curves (specimens of 16-mm-diameter rebars)

Fig. 22
figure 22

Analytical versus experimental bond–slip curves (specimens of 22-mm-diameter rebars)

This comparison showed a high deviation between the experimental results with those obtained analytically from the aforementioned two models. This means that, these models are of low accuracy to predict the bond behavior of AASC which attributed to the difference between the conventional concrete and the AASC in many aspects such as components, hydration products, manufacturing technique and general behavior. That is why a modified model is proposed to predict AASC bond behavior with a higher accuracy.

4.3 Proposed Modified Model

The main target of this analytical study was to introduce a proposed modified model in order to predict a complete bond behavior between ambient cured AASC and steel rebars more accurate than the aforementioned models used for conventional concrete.

To improve the prediction level of AASC bond behavior, modifications were proposed on the main parameters of CEB-FIP model based on the technique of best fitting for the obtained experimental results, these modifications are shown in Table 12. These modifications were in the bond strength (\(\tau_{{{\text{max}}}}\)) and the characteristic slippage (\(S_{3}\)). The bond strength increased from \(2 \sqrt {f^{\prime}_{c} }\) to \(2.5 \sqrt {f^{\prime}_{c} }\), as the AASC showed bond strength higher than the conventional concrete as reported in the literature and as obtained from the experimental results of this research work. The characteristic slippage (\(S_{3}\)) modified from 1.00 mm to the clear rib spacing of rebars to make the descending branch less steep.

Table 12 Modified defining parameters of the bond stress–slippage relationship

Comparison between the results of proposed model, and both of the obtained experimental results and the results obtained analytically from the aforementioned two models was conducted at both ambient temperature (25 °C) and elevated temperatures of 300 °C and 600 °C as shown in Figs. 23, 24 and 25, respectively. It was noted that the proposed modified model matched well the experimental results at ambient temperature (25 °C). This can be attributed to that the criteria used in the study to modify the model were based on the findings of previous studies conducted on AAC samples at ambient temperature, due to the limited studies found for elevated temperatures. Also, it was observed that the proposed modified model gave over-estimated bond–slip relationships for all specimens that were exposed to elevated temperatures except 12-mm-diameter rebars specimens, which the proposed modified model matched well their ascending branches up to the maximum bond strength and then gave over-estimated descending branches. This means that there is a need for further investigation to reach a modification factor for the main parameters of the bond–slip relationship, especially for \(\tau_{{{\text{max}}}}\) and S3, to be used in the case of exposure to elevated temperatures. After considering the results obtained from this study, this factor is likely to be a reduction factor. Also, it is recommended for this modification factor to be linked to the used rebars diameter.

Fig. 23
figure 23

Proposed analytical versus experimental bond–slip relationships (ambient temperature of 25 °C)

Fig. 24
figure 24

Proposed analytical versus experimental bond–slip relationships (elevated temperature of 300 °C)

Fig. 25
figure 25

Proposed analytical versus experimental bond–slip relationships (elevated temperature of 600 °C)

5 Conclusions

Both of experimental and analytical investigation for the bond behavior between AASC and steel rebars after exposing to elevated temperatures was presented and discussed. Based on analyzing and discussing the obtained results, the following conclusions can be drawn:

  • Failure mode for all beam-end specimens was by splitting. There was no significant difference observed in the obtained cracking pattern or failure mode due to exposing to the elevated temperatures.

  • The degradation level of bond strength after exposing to elevated temperatures above 300 °C was significant. Generally, bond strength decreased, and corresponding slippage increased due to the elevated temperatures exposure.

  • Based on the obtained signal-to-noise (S/N) ratios, participation percentages and optimum levels of each considered parameters, the bond strength decreased with increasing the rebar diameter and increased slightly with increasing the L/d ratio.

  • The CEB-FIP model provided more conservative values for bond strength compared to the experimental results which increase the safety level when estimating bond strength in design purposes.

  • The proposed modified model achieved a higher correlation with the obtained experimental results than CEB-FIP model at ambient temperature.

Availability of data and materials

All data generated or analyzed during this study are included in this published article.

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Ismail Amer: resources, investigation, validation, visualization, writing—original draft. Mohamed Kohail: writing—review and editing, validation, conceptualization, methodology. M.S. El-Feky: writing—review and editing, validation, conceptualization, methodology. Ahmed Rashad: conceptualization, methodology, supervision. Mohamed A. Khalaf: writing—review and editing, supervision. All authors read and approved the final manuscript.

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Ismail Amer: Assistant Professor, Structural Engineering Department, Faculty of Engineering, Ain Shams University, Egypt. Mohamed Kohail: Associate Professor, Structural Engineering Department, Faculty of Engineering, Ain Shams University, Egypt. M.S. El-Feky: Associate Professor, Civil Engineering Department, National Research Centre, Egypt. Ahmed Rashad: Associate Professor, Structural Engineering Department, Faculty of Engineering, Ain Shams University, Egypt. Mohamed A. Khalaf: Professor, Structural Engineering Department, Faculty of Engineering, Ain Shams University, Egypt.

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Correspondence to Mohamed Kohail.

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Amer, I., Kohail, M., El-Feky, M.S. et al. Realistic Evaluation of Reinforcement Bond Strength in Alkali-Activated Slag Concrete Exposed to Elevated Temperature. Int J Concr Struct Mater 17, 36 (2023). https://doi.org/10.1186/s40069-023-00596-2

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